ST PETERSBURG TABLE OF CONTENTS

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13. Connect a full cylinder of technical grade nitrogen to valve (VB 763) using a high flow regulator (Harris 3500 series regulators work well) NOTE: Once nitrogen purge is preformed take care not to allow air back into the system. 14. Open valve (VB 763) 15. Open the nitrogen cylinder valve and adjust the regulator in 16. Continue to fill the vessels until pressure gauges (PI 361 and PI 362) read 5 psi 17. Close the nitrogen cylinder valve and adjust the regulator all the way out 18. Let the nitrogen stand in the vessels for 5 minutes 19. Open valve (VB 362) to purge the nitrogen from the vessels 20. Close valve (VB 362) 21. Repeat steps 15 thru 20 two more times 22. Close valve (VB 763) 23. Unhook the nitrogen tank and regulator 24. Open the filter housing on carbon particulate filter (FLT 363) 25. Clean or replace the filter element as necessary 26. Re-install the filter housing on the carbon particulate filter 27. Open valves (VB 352 and VB 364) 28. Re-energize and re-start the skid Section 8 Siloxane Page 5

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